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This laboratory manual introduces students to modern synthetic and instrumental techniques currently used in inorganic chemistry. The third edition has been updated to reflect developments in the field, providing greater emphasis on applications related to biochemistry and materials science.- CONTENTS.: Introduction; Safety; Laboratory Procedures; Research Notebook; Standard References Part I. Solid State Chemistry Experiment 1 – High-Temperature Synthesis of the Superconductor YBa2Cu3O7 Tube Furnace PreparationSuperconductivityIodometric Titrations Experiment 2 – The Layered Solids VOPO4(H2O)2 and VO(HPO4)(H2O)0.5 Powder X-Ray DiffractionOxidation of Alcohols to Ketones Experiment 3 – The Molecular Sieve Zeolite-X Sol-gel SynthesisHigh Pressure SynthesisIon Exchange in Microporous Solids Part II. Main Group Chemistry Experiment 4 – The Borane-Amine Adduct BH3NH2C(CH3)3 Lewis Acids and Bases Experiment 5 – Buckminsterfullerene, C60, and Its Electrochemistry Soxhlet ExtractionCyclic Voltammetry Experiment 6 – Vacuum-Line Synthesis of GeH4 Vacuum Line and Trap-to-Trap PurificationVapor Pressure and Molecular Weight Determination of a Volatile CompoundGas Phase IR Spectroscopy Experiment 7 – Tin Chemistry: Coordination Complexes and Organometallic Derivatives NMR SpectroscopyLinkage Isomerism Experiment 8 – Synthesis of (C6H5)2PCH2CH2P(C6H5)2 in Liquid Ammonia Synthesis in Liquid Ammonia Experiment 9 – Electrolytic Synthesis of K2S2O8 Electrolytic Preparation Part III. Coordination Chemistry Experiment 10 – Ion Exchange Separation of Chromium Complexes Ion Exchange Chromatography Experiment 11 – Metal-Metal Quadruple Bonds Molecular Orbital Theory Experiment 12 – The Magnetic Susceptibility of Mn(acac)3 Magnetism of Transition Metal ComplexesThe Gouy MethodThe Evans Methods Experiment 13 – Cobalt Ammines and their Ligand Substitution Kinetics Conductivity of Ionic ComplexesKinetics of Aquation of [Co(NH3)5Cl]2+ Experiment 14 – Optical Resolution of Co(en)33+ Separation of Diastereomers by CrystallizationOptical RotationsSuction Filtration Experiment 15 – Metal Dithiolenes and the Use of Quaternary Ammonium Salts Quaternary Ammonium Salts Part IV. Organometallic Chemistry Experiment 16 – The Metal-Arene Complex [1,3,5-C6H3(CH3)3]Mo(CO)3 IR Spectra of Metal Carbonyls Experiment 17 – Organo-iron Chemistry: (C5H5)2Fe2(CO)4 and (C5H5)Fe(CO)2(CH3) Schlenk Line SynthesisInfrared Spectra of Solutions Experiment 18 – The Metal Carbonyl Cluster Fe3(CO)12 Mass Spectrometry Experiment 19 – Microscale Synthesis of Vaska’s Complex Microscale SynthesisSolid State IR Spectra Experiment 20 – The Air-Sensitive Sandwich Complex Nickelocene Glove Bag ManipulationsSublimation Part V. Bioinorganic Chemistry Experiment 21 – Cobaloximes: Models of Vitamin-B12 Coenzymes Enzyme Models Experiment 22 – Amino Acid Complexes: Stability Constants of Ni(glycinate)n(2 – n)+ Amino Acid ChemistrypH TitrationspKa and Successive Stability Constant Determination Experiment 23 – Bioinorganic Coordination Chemistry: Copper (II) Tetraphenylporphyrinate Porphyrin ChemistryThin-Layer ChromatographyColumn ChromatographyNotes to the Instructor; Appendices; NMR and Mass Spectra; Index

por Gregory S Girolami (Autor) – 1999

  • Capa comum ‏ : ‎ 280 paginas
  • ISBN-10 ‏ : ‎ 0935702482
  • ISBN-13 ‏ : ‎ 9780935702484
  • Obs.: Livro sem uso, com paginas amareladas e um pouco sujas pelo tempo – capa, contracapa, bordas e paginas integras. sem marcas, grifos, marcações ou qualquer tipo de detalhe que possa interferir na leitura ou pesquisa – Conteudo perfeito

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